Steel Tempering: Factors, Techniques, and Treatments

Factors Affecting Steel Tempering

Several factors influence the achievement of optimal steel tempering, including:

  • Steel type and structural state
  • Thermal conductivity
  • Part size
  • Cooling medium

The initial structure’s grain size affects the critical cooling speed; larger grains slow down austenite transformation.

Hardenability

Hardenability refers to steel’s ability to achieve depth of hardening, not its toughness. Methods for measuring hardenability include:

  • Impact fracture observation
  • Acid etching to reveal structures
  • Hardness variation studies (most accurate)

Jominy Test

Standardized Hardenability Assessment

The Jominy test (adopted by AISI and SAE) determines crucial steel characteristics, especially for setting property boundaries in standard steels. This test provides information on:

  • Minimum and maximum achievable hardness
  • Hardenability
  • Cooling media effects

Jominy discovered a direct correlation between tensile mechanical properties and steel hardness.

Steel Tempering Techniques

Cooling Methods

Common cooling media include:

  • Water: Its low boiling point can reduce cooling speed.
  • Oil: Mineral-based oils with viscosities between 5 and 9 degrees are typical.
  • Mercury: Used for special cases requiring extreme hardness, despite its high cost.

The cooling process involves three steps:

  1. Heat loss by conduction and radiation through the gaseous layer.
  2. Vapor transport cooling, influenced by bath viscosity and cracking potential.
  3. Cooling by conduction and convection in the liquid.

Patenting

Isothermal Transformation for High-Tensile Wire

Patenting is used before or during high-tensile wire drawing. It involves heating the wire to full austenitization, then cooling it in a molten lead bath (350-600°C). This isothermal annealing process requires careful temperature control.

Austenmpering

Tempering for Tools and Small Parts

Austenmpering is effective for tools and small steel parts, minimizing fissures and tensions associated with martensitic structures. It is less economical for large pieces.

Martenpering

Stress Reduction in Hardening

Martenpering aims to achieve martensitic hardening while eliminating stress cracks. This is done by cooling the austenitized metal in a molten salt bath (200-300°C). It’s used for manufacturing bearings, gears, etc.

Post-Tempering Treatments

Tempering

Complementary Annealing

Tempering is a complementary annealing process following quenching. Quenching to achieve a martensitic structure can induce internal tensions. Tempering improves mechanical properties by adjusting annealing temperature and duration.

Surface Treatments

Enhancing Toughness and Wear Resistance

Surface treatments with varying compositions are used for parts requiring both toughness and high hardness/wear resistance. This is achieved by combining low-carbon steels (for toughness) with high-alloy steels (for hardness). Common methods include:

  • Cementation
  • Carbonitriding
  • Sulfanization